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- W2034149062 abstract "Heptaphosphane(3) (1) is obtained pure by the reaction of (Me 3 Si) 3 P 7 with methanol and has been characterized NMR spectroscopically (in nascent state). It turned out to be a mixture of two diastereomers P 7 H 3sym and P 7 H 3asym , which differ in the spatial arrangement of the hydrogen atoms. Both isomers were proven to possess the earlier reported structure of a tri-cyclo[2.2.1.0 2,6 ]heptaphosphane, which in the case of P 7 H 3sym was ascertained by a complete analysis of its 31 P{ 1 H} NMR spectrum. As shown by the chemical shifts, the P 7 cage in P 7 H 3sym is clearly stretched compared with P 7 Me 3sym and (Me 3 Si) 3 P 7 ." @default.
- W2034149062 created "2016-06-24" @default.
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- W2034149062 date "1985-11-01" @default.
- W2034149062 modified "2023-09-28" @default.
- W2034149062 title "Beiträge zur Chemie des Phosphors, 161 [1] Kernresonanzspektren und Struktur von Heptaphosphan(3), P<sub>7</sub>H<sub>3</sub> / Contributions to the Chemistry of Phosphorus, 161 [1] NMR Spectra and Structure of Heptaphosphane(3), P<sub>7</sub>H<sub>3</sub>" @default.
- W2034149062 doi "https://doi.org/10.1515/znb-1985-1102" @default.
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