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- W2034170260 abstract "A laboratory working procedure is described for silanization of glass capillaries with bis(cyanopropyl)tetramethyldisiloxane, prior to coating with XE-60-L-valine-(S)-α-phenylethylamide as chiral stationary phase. GC columns thus prepared exhibit good inertness and no long-term deterioriation of enantioselectivity up to 220°C. A general procedure is given for derivatization of simple and of polyfunctional amino acids, in a batch mixture, simultaneously, and completely at both the N- and the C-terminus and all other protic functions. Within the seven series of N-pivaloyl amino acid esters tested (methyl to neopentyl), baseline separation is obtained for all R/S pairs, including the proline derivative." @default.
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- W2034170260 date "1989-04-01" @default.
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- W2034170260 title "Systematic investigation of enantiomer resolution ofN-pivaloyl derivatized amino acid esters. Preparation of glass capillary columns coated with the chiral phase XE-60-L-val-pea" @default.
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- W2034170260 doi "https://doi.org/10.1002/jhrc.1240120405" @default.
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