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- W2034170894 abstract "Heating trichlorosilane with conjugated dienes or an acetylene solution at 150 or 180 °C in the presence of a catalytic quantity of tetrabutylphosphonium chloride resulted in elimination of HCl and dichlorosilylene transfer to the unsaturated substrates to afford silacyclopentenes or 1,4-disilacyclohexa-2,5-dienes, respectively, in good to excellent yields. The trapping reaction with hex-3-yne gave 1,1,4,4-tetrachloro-2,3,5,6-tetraethyl-1,4-disilacyclohexa-2,5-diene in 79% yield, and its structure was determined by X-ray crystallography." @default.
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- W2034170894 date "2003-05-17" @default.
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- W2034170894 title "Phosphonium Chloride Induced Dichlorosilylene Transfer from Trichlorosilane" @default.
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- W2034170894 doi "https://doi.org/10.1021/om0302488" @default.
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