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- W2034172281 abstract "An HPLC/MS/MS method was validated for the low level analysis of pyridostigmine bromide (PB) from guinea pig plasma. An advantage of this strong-cation exchange HPLC/MS/MS method was the enhancement of the ESI-MS signal by providing good retention and good peak shape of PB with a mobile phase of 70% acetonitrile. In addition, the use of 70% acetonitrile in the mobile phase allowed the direct injection of the supernant from the protein precipitated extracted sample. The assay was linear from the range of 0.1 to 50 ng/ml using only 25 microl of sample. The precision and accuracy of the assay was better than 9.1 and 113%, respectively." @default.
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- W2034172281 date "2003-11-01" @default.
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- W2034172281 title "Development and validation of a liquid chromatography–tandem mass spectrometry method for the determination of pyridostigmine bromide from guinea pig plasma" @default.
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- W2034172281 doi "https://doi.org/10.1016/j.jchromb.2003.08.021" @default.
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