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- W2034185330 abstract "Mo8O23 is incommensurately modulated between the temperatures 285 K and 360 K. In this article results are presented on the determination of the structure of this compound at 298 K. The monoclinic cell parameters are determined to be a=13.382(1) AA, b=4.0519(6) AA, c=16.877(2) AA and beta =106.197(3) degrees . The space group of the average structure is found to be P2/c, in accordance with previous studies. The observed satellite reflections can be indexed using a single modulation wavevector, which has components (0.188, 0.5, 0.133). The superspace group characterising the symmetry of the incommensurately modulated structure is B11P2C/. Refinement on 6270 main reflections and 1940 satellites, with I>2.5 sigma (I), gave convergence to a weighted R-factor of 0.029, with partial R-factors of 0.024 for main reflections and 0.095 for satellite reflections. The modulation is interpreted as a combination of rotations and distortions of the MoO6 octahedra." @default.
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- W2034185330 date "1990-01-08" @default.
- W2034185330 modified "2023-09-26" @default.
- W2034185330 title "Determination of the incommensurately modulated structure of Mo<sub>8</sub>O<sub>23</sub>by means of single-crystal X-ray diffraction" @default.
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- W2034185330 doi "https://doi.org/10.1088/0953-8984/2/1/003" @default.
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