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- W2034191451 endingPage "311" @default.
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- W2034191451 abstract "Current methods are reviewed for determining the position of double bonds in fatty acids, and other unsaturated organic compounds, using mass spectrometry. ‘On-site’ and ‘remote-site’ derivatization methods are described, and their advantages and disadvantages for mass spectrometric analysis discussed. Chemical transformation of double bonds by methoxylation, silyloxylation or deuteration, together with electron impact (EI), chemical ionization (CI) or collisionally induced decomposition (CID) techniques in combination with fast atom bombardment (FAB) or CI, are found to be most suitable for polyunsaturated fatty acids (PUFA): for the analysis of less unsaturated compounds on a submicrogram scale those methods are most promising which either do not involve derivatization of the double bonds, or give derivatives in quantitative yields. Effects of mass spectrometer geometry and operating conditions are also considered." @default.
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- W2034191451 date "1986-03-01" @default.
- W2034191451 modified "2023-10-12" @default.
- W2034191451 title "Mass spectrometric localization of carbon-carbon double bonds: A critical review of recent methods" @default.
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- W2034191451 doi "https://doi.org/10.1016/0009-3084(86)90112-x" @default.
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