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- W2034192103 abstract "Electron-deficient pyrrole (1) was derivatized by diazotization with p-nitrobenzene diazonium chloride. Reduction of the diazo intermediates gave 2- and 1-aminopyrroles (3 and 4). The 2-aminopyrrole (3) was determined to be the process impurity formed during a furan−pyrrole heteroatom exchange reaction. An oxidative mechanism for the impurity formation was hypothesized. Nitrogen sparging of the reaction mixture prior to heating eliminated formation of 3." @default.
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- W2034192103 date "2001-10-17" @default.
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- W2034192103 title "Structural Determination of a Process Impurity in a Furan−Pyrrole Heteroatom Exchange Reaction" @default.
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- W2034192103 doi "https://doi.org/10.1021/op010227u" @default.
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