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- W2034215322 abstract "The copper(II), nickel(II) and silver(I) complexes of the pentadentate 17-membered macrocycle 1, 12, 15-triaza-3, 4:9, 10-dibenzo-5,8-dithiacycloheptadecane (L1) have been prepared as perchlorates and characterized by X-ray crystallography. The N3S2 ligand uses all donor atoms for complexation. The copper coordination is square pyramidal with one sulfur atom in the axial site. Ni(II) displays an octahedral coordination by an interaction with a water molecule. The Ag(I) coordination is best described as a distorted pentagonal bipyramid. In [CuL1]2+ the 1, 4, 7-triazaheptane fragment of L1 is meridionally coordinated, but facially in [NiL1(H2O)]2+ and intermediate in [AgL1](ClO4). Crystal data for [CuL1](ClO4)2: monoclinic, space group P21/n, a = 13.153(8), b = 11.951(5), c = 17.880(8)Å, β = 110.29(4)°, Z = 4, R = 0.086 for 2732 independent reflections with I ⩾ 2σ(I); [NiL1(H2O)](ClO4)2: monoclinic, P21/a, a = 10.771(2), b= 16.157(2), c = 15.286(2) Å, β =93.08(1)°, Z = 4, R = 0.085 for 1464 independent reflections with I ⩾ 2σ(I); [AgL1](ClO4): monoclinic, P21/n, a = 12.708(9), b = 9.483(7), c = 19.569(13) Å, β= 103.95(6)°, Z = 4, R = 0.039 for 3600 independent reflections with I ⩾ 2σ(I)." @default.
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- W2034215322 date "1991-02-01" @default.
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- W2034215322 title "X-ray crystal structures of the copper(II), nickel(II) and silver(I) complexes of a 17-membered dibenzo macrocycle with a N3S2 donor set" @default.
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- W2034215322 doi "https://doi.org/10.1016/s0020-1693(00)84942-7" @default.
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