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- W2034229634 abstract "A solid-phase microextraction (SPME) analytical method has been developed for the determination of N-nitrosodi-n-butylamine (NDBA) and N-nitrosodibenzylamine (NDBzA) in hams that is based on: (a) isolation of the compounds by steam distillation, (b) SPME from the distillate headspace using a polycrylate coated silica fibre and (c) determination by gas chromatography-thermal energy analyzer technique or confirmation by gas chromatography-mass spectrometry. Recoveries of both NDBA and NDBzA from hams spiked at 5 to 160 μg/kg levels ranged between 41 to 112%. The overall method is fast, sensitive (detection limits, 1 to 3 μg/kg), precise (within 10%) and fairly accurate (average recoveries 86% and 70%, respectively). The results obtained by this technique for seven ham samples agreed fairly well with those obtained by an existing method (r2 = 0.97). The new method is solventless, environmetally friendly and useful for rapid monitoring purposes." @default.
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- W2034229634 title "Rapid semi-quantitative estimation of N-nitrosodibutylamine and N-nitrosodibenzylamine in smoked hams by solid-phase microextraction followed by gas chromatography-thermal energy analysis" @default.
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- W2034229634 doi "https://doi.org/10.1016/s0021-9673(97)00716-4" @default.
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