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• W2034245076 abstract "MgCl2·6H2O, MgBr2, MgI2, FeCl2, NiCl2 and dppp {1,3-bis(diphenyl-phosphine)propane} react with Hg(SePh)2 in dimethylformamide (dmf) to give the new cluster compounds [M(dmf)6][Hg8SeX4(PhSe)12] {M = Mg2+: X = Cl (1a), Br (1b), I (1c); for M = Fe2+ (2) and Ni2+ (3), X = Cl}. All the clusters show the presence of [μ-Se] bridges, achieved by all the [SePh]− groups. Compound 3 reproduces with selenium an earlier reported tellurium cluster. In the anions [Hg8SeX4(PhSe)12]2− the eight Hg atoms exhibit a distorted square antiprismatic assembly with a four-coordinated μ4-Se atom in the center, in an ideal tetrahedral arrangement. The counter ions [M(dmf)6]2+ attain perfect octahedral geometries, with the three octahedral axis presenting exactly 180°. The use of intermediary ligands and their synthetical utilities will discussed, as well as some optical features of the title compounds." @default.
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• W2034245076 date "2012-03-01" @default.
• W2034245076 modified "2023-10-16" @default.
• W2034245076 title "On the synthesis and structure of HgSe clusters: Synthetic–structural considerations and optical features of new cluster compounds" @default.
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• W2034245076 doi "https://doi.org/10.1016/j.poly.2012.01.006" @default.
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