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• W2034281056 abstract "Solid-state 13C cross polarization magic angle spinning nuclear magnetic resonance measurements on β-cyclodextrin (β-CD)/substituted aromatic ketone inclusion complexes indicate that the interaction between the β-CD (host) and the substituted ketone (guest) depends markedly on the substituent. The carbon chemical shifts of both the host and the guest molecules depend on the substituent. In the β-CD/α-aminoacetophenone complex, each carbon of the guest molecule exhibits two 13C NMR peaks. One of these peaks is shifted with respect to that of the free molecule. This shifted peak gradually disappears when the temperature increases, whereas the unshifted peak is unchanged. The same phenomenon occurs when the inclusion complex is washed. This result is related to the existence of two kinds of complexed molecule (inside the β-CD cavity and outside but non-covalently bonded to β-CD). In β-CD/α-amino-4-bromoacetophenone, only one kind of complexed molecule exists. The disposition of α-amino-4-bromoacetophenone inside the β-CD cavity is different from that of α-aminoacetophenone." @default.
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• W2034281056 date "1996-08-01" @default.
• W2034281056 modified "2023-09-25" @default.
• W2034281056 title "Solid-state 13C NMR study of β-cyclodextrin/substituted aromatic ketone complexes: evidence for two kinds of complexation of the guest molecules" @default.
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• W2034281056 doi "https://doi.org/10.1016/0927-7757(96)03614-x" @default.
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