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- W2034302022 abstract "Solid state lithium batteries are very promising power sources. However, many problems concerning lithium insertion/extraction are yet to be resolved. Tin-indium mixed valence sulfides with spinel structure have been used as lithium insertion host-matrix. The chemical way via n-butyllithium has been chosen for its softness. Atomic emission spectroscopy reveals the time dependence of the reaction. X-ray diffraction shows that the reaction is topotactic. An electronic transfer SnIV ⇄ SnII is evident from 119S n Mössbauer spectra. The knowledge of the Lamb-Mössbauer factors of SnIV and SnII allows the evaluation of the SnIV quantity reduced further to lithium insertion and then, the amount of lithium taking part in this process. The results lead us to the inclusion of a second oxidoreduction mechanism InIII ⇄ InI. 7Li N.M.R. analysis reveals a double-line subspectra related to two types of lithium with different mobilities." @default.
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- W2034302022 date "1993-10-01" @default.
- W2034302022 modified "2023-09-27" @default.
- W2034302022 title "Time-dependent lithium insertion in mixed valence tin, indium sulfide spinels. Tin Mössbauer spectroscopy and lithium N.M.R." @default.
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- W2034302022 doi "https://doi.org/10.1016/0025-5408(93)90147-6" @default.
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