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• W2034320524 abstract "Abstract MoO 3 /γ‐Al 2 O 3 composites are synthesized by CVD under atmospheric pressure using Mo(CO) 6 as the precursor and porous γ‐Al 2 O 3 particles in a horizontal, rotating, hot‐wall reactor, which is also used for calcination in air. The composites are characterized by N 2 physisorption, atomic absorption spectroscopy, X‐ray photoelectron spectroscopy (XPS), X‐ray diffraction (XRD), transmission electron microscopy (TEM), and laser Raman spectroscopy (LRS). The synthesized samples exhibit excellent porosity, even at high Mo loadings. A much higher Mo yield is achieved when applying sublimation‐adsorption in static air instead of using flowing N 2 . A high degree of Mo dispersion on alumina is confirmed by XRD, LRS, and TEM; with a Mo surface density as high as 5.2 atoms nm −2 , the sample is X‐ray amorphous, there are no polymeric molybdate species detectable by LRS, and the island size of the molybdate species is about 1 nm according to TEM. The XPS analysis shows that exclusively Mo VI species are present on all synthesized samples. Thus, the applied rotating, hot‐wall reactor achieves efficient mixing and homogeneous deposition." @default.
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• W2034320524 date "2011-05-26" @default.
• W2034320524 modified "2023-10-08" @default.
• W2034320524 title "Highly Dispersed MoO₃/Al₂O₃ Shell‐Core Composites Synthesized by CVD of Mo(CO)₆ under Atmospheric Pressure" @default.
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• W2034320524 doi "https://doi.org/10.1002/cvde.201106909" @default.
• W2034320524 hasPublicationYear "2011" @default.
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