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- W2034325071 abstract "Tetraethoxysilane-derived silica containing lithium and manganese nitrates has been prepared in solutions of poly(oxyethylene) surfactants, giving novel monolithic gels in which the metal ions are associated with the incorporated surfactant. Calcination produces nanocrystalline lithium manganate in the silica matrix. The gels and calcined phases have been characterized by X-ray diffraction and X-ray absorption near edge and extended fine structure spectroscopy at the Mn K-edge (XANES and EXAFS). At 400 °C the reaction between lithium and manganese is incomplete, and both nanocrystalline lithium manganate and disordered manganese in a lower-valent state are identified. Including excess lithium in the gels and calcining at 500 °C allows practically all the manganese in the gels to be reacted to form lithium manganate phases with manganese in a predominantly tetravalent oxidation state. Electron microscopy shows that different microstructures and particle morphologies are obtained by varying the nature and c..." @default.
- W2034325071 created "2016-06-24" @default.
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- W2034325071 date "1997-12-01" @default.
- W2034325071 modified "2023-10-18" @default.
- W2034325071 title "Nanoscale Control of the Morphology of Lithium Manganate and Silica Composites Using Self-Organized Sol−Gel Media" @default.
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- W2034325071 doi "https://doi.org/10.1021/cm9705698" @default.
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