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• W2034334283 endingPage "012010" @default.
• W2034334283 startingPage "012010" @default.
• W2034334283 abstract "Thallium is a toxic metal that introduced into the environment mainly as a waste from the production of zinc, cadmium, and lead and by combustion of coal. Thallium causes gastrointestinal irritation and nerve damage when people are exposed to it for relatively short period of time. For long term, thallium has the potential to cause the following effects: change in blood chemistry, damage to liver, kidney, intestinal and testicular tissue, and hair loss. In this work a membrane was prepared by use of 4'–nitrobenzo –18–crown–6 (4'NB18C6) as an ion carrier, polyvinylchloride (PVC) as a matrix, and diocthylphetalate (DOP) as a plasticizer for making an ion selective electrode for measurement of Tl+ cation in solutions. The amount of 4'-nitrobenzo-18C6 and polyvinylchloride were optimized in the preparation of the membrane. The response of the electrode was Nernstian within the concentration range 1.0 × 10−8 to 1.0 × 10−1M. This sensor displays a drift in Nernstian response for this cation with increasing the amount of ionophore and decreasing the amount of polyvinylchloride.The results of potentiometric measurements showed that, this electrode also responses to Cu2+ Ni2+ and Pb2+ cations, but the electrode has a wider dynamic range and a lower detection limit to Tl+ cation. The effects of various parameters such as pH, different cations interferences, effect of the amount of ionophore and polyvinylchloride and time on response of the coated ion selective electrode were investigated. Finally the constructed electrode was used in complexometric and precipitation titrations of Tl+ cation with EDTA and KBr, respectively. The response of the fabricated electrode at concentration range from 1.0 × 10−8 to 1.0 × 10−1M is linear with a Nernstian slope of 57.27 mV." @default.
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• W2034334283 date "2011-02-01" @default.
• W2034334283 modified "2023-10-01" @default.
• W2034334283 title "A Novel Ion – selective Polymeric Membrane Sensor for Determining Thallium(I) With High Selectivity" @default.
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• W2034334283 doi "https://doi.org/10.1088/1757-899x/17/1/012010" @default.
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