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- W2034340686 abstract "Abstract The structure consists of singly charged 3-amino-1- propylammonium cations and tetrahedral perchlorate counterions. Both of the terminal N atoms form three N--H bonds, each of which is involved in a strong hy- drogen bond [N...O 2.739 (5)-2.845 (5) ,~]. This requires the lone proton to partially occupy sites on both N atoms, thereby giving each some ammonium character. diperchlorate (Pritchard et al., 1992). However, compar- ison of the perchlorate anions in the two salts shows a significant bond lengthening in the title compound [1.456(3)-1.478(3), average 1.471 .~, compared with 1.406 (4)-1.445 (4), average 1.425 ,A,]. This is related to improved hydrogen bonding in the monoperchlorate, where five H atoms (disordered over six sites) form hydro- gen bonds with N...O separation 2.739 (5)-2.845 (5) compared with 2.95 (1)-3.23 (1) ,~ for the diammonium salt. The title structure also differs from ammonium per- chlorate (Lundgren, 1979) and monomethylammonium perchlorate (Zanazzi, 1968) in this respect, both of which have shorter C1--O bonds and longer, weaker hydrogen bonds. Experimental" @default.
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- W2034340686 date "1993-09-15" @default.
- W2034340686 modified "2023-10-18" @default.
- W2034340686 title "3-Amino-1-propylammonium perchlorate: an extensively hydrogen-bonded system" @default.
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- W2034340686 doi "https://doi.org/10.1107/s010827019300277x" @default.
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