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- W2034346927 abstract "Electrochemistry has been introduced as a powerful tool in order to prepare new organometallic reagents for functionalizing of mesoporous silica. Preparation of the reagents was based on electrochemical oxidation of dihydroxybenzene derivatives in the presence of 3-(trimethoxysilyl)-1-propanethiol as a nucleophile. The mechanisms of electrochemical reactions were studied by voltammetric studies. Mesoporous silica SBA-15 was also synthesized in this work through sol-gel hydrothermal method using Genapol PF-10 as structure directing compound. The prepared mesoporous silica was characterized by FT-IR analysis and Barrett–Joiner–Halenda (BJH) pore size and Brunauer–Emmett–Teller (BET) surface area measurement methods using N 2 adsorption–desorption isotherm. Finally, the organometallic reagent was covalently grafted on the surface of mesoporous silica. Functionalizing of this material with the new reagent was confirmed by Fourier transform infrared (FT-IR) spectroscopy. The functionalized mesoporous silica by new reagent can be utilized in biological applications." @default.
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- W2034346927 date "2013-05-28" @default.
- W2034346927 modified "2023-10-16" @default.
- W2034346927 title "ELECTROCHEMICAL PREPARATION OF NEW ORGANOSILICONE COMPOUNDS FOR FUNCTIONALIZING OF MESOPOROUS SILICA" @default.
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- W2034346927 doi "https://doi.org/10.1142/s1793604713500318" @default.
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