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- W2034358635 abstract "The reaction of methyl (5-acetamido-4,7,8,9-tetra-O-acetyl-2,3,5-trideoxy-d- glycero-β-d-galacto-2-nonulopyranosyl chloride)onate with benzyl 2-azido-3,4-di- O-benzyl-2-deoxy-β-d-galactopyranoside promoted by mercury cyanide-mercury bromide afforded a 1:1 mixture of the two anomeric (2→6)-linked disaccharides containing N-acetylneuraminic acid. Chromatography gave 42% of benzyl 2-azido- 3,4-di-O-benzyl-2-deoxy-6-O-[methyl-(5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-di deoxy-d-glycero-α-d-galacto-2-nonulopyranosyl)onate]-β-d-galactopyranoside and 36% of the corresponding β-d-(2→6)-linked isomer. A deblocking sequence led to 2-acetamido-6-O-(5-acetamido-3,5-dideoxy-d-glycero-α-d-galacto-2-nonulopyranosylonic acid)-2-deoxy-d-galactopyranose and to the corresponding β-d-(2→6)-linked compound. The anomeric configurations were assigned by use of 2D-N.m.r.-spectroscopy." @default.
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- W2034358635 date "1985-03-01" @default.
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- W2034358635 title "Synthese einer disaccharideinheit aus N-acetylneuraminsäure und 2-acetamido-2-desoxy-d-galactose" @default.
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- W2034358635 doi "https://doi.org/10.1016/0008-6215(85)85149-1" @default.
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