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- W2034372723 abstract "The binuclear cyclopalladated compounds [Pd2(μ-OH)2(Ln)2] (1) derived from imines HLn = p-CnH2n + 1O–C6H4–CHN–C6H4–OCnH2n + 1-p (n = 6,10) react with carboxylic acids to give the derivatives [Pd2(μ-ox)2(Ln)2] (2) with a planar core for oxalic acid, and [Pd2(μ-OOCR)2(Ln)2] (3–7) compounds with a non-planar ridge tent structure for other RCOOH acids: (3) R = CmH2m + 1 (m = 1, 3, 5, 7, 9, 11, 13, 15, 17); (4) R = CH2(OCH2CH2)pOCH3 (p = 1, 2); (5) R = CH2–C6H4–OCqH2q + 1-p (q = 2, 4, 6, 8, 10, 12); (6) R = C6H4–OCrH2r + 1-p (r = 4, 10); (7) R = C*H(OH)CH3. The acids used were designed to explore the effect on the thermal properties of the compounds prepared of systematic variations in the type of carboxylato ligand, which induce structure, packing, and polarity changes, and in the length of the carboxylato chain. Most of the complexes prepared, even when far from planar, show liquid crystal behavior and display nematic, smectic A and smectic C phases." @default.
- W2034372723 created "2016-06-24" @default.
- W2034372723 creator A5000819530 @default.
- W2034372723 creator A5003144448 @default.
- W2034372723 creator A5005749039 @default.
- W2034372723 creator A5059093565 @default.
- W2034372723 date "2005-01-01" @default.
- W2034372723 modified "2023-09-27" @default.
- W2034372723 title "Mesogens based on palladium orthometallated complexes with carboxylato bridges: tuning and shaping a non-planar molecule" @default.
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- W2034372723 doi "https://doi.org/10.1016/j.jorganchem.2004.09.024" @default.
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