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- W2034452426 abstract "Treatment of 6-amino-1,3-dimethyl-5-nitrosouracil (Ia) with dimethyl acetylenedicarboxylate (DMAD) in dimethylformamide (DMF) afforded 6,7-bis(dimethoxycarbonyl)-1,3-dimethyllumazine (II). Similarly, the reaction of 6-amino-1,3-dimethyl-5-phenylazouracil with DMAD gave also II. Hydrolysis of II with hydrochloric acid gave 1,3-dimethyllumazine-6-carboxylic acid (III). III was chlorinated with thionyl chloride and then aminated with ethanolic ammonia to give rise to 6-carbamoyl-1,3-dimethyllumazine (V). V was alternatively synthesized by the treatment of Ia with propiolamide in DMF." @default.
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- W2034452426 date "1982-07-01" @default.
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- W2034452426 title "A synthesis of lumazine derivatives" @default.
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- W2034452426 doi "https://doi.org/10.1002/jhet.5570190452" @default.
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