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- W2034578045 startingPage "3076" @default.
- W2034578045 abstract "The title rotational isomers were synthesized. Reduction of methyl 2-(9-anthryl)-2-methylpropanoate caused difficulty due to severe steric effects. Thus the compound was converted to the free acid by treating it with a lithium thiolate and the resulted acid was reduced to the corresponding alcohol with borane. The alcohol was protected as either an acetate or a silyl ether and was subjected to the reaction with a benzyne. The resulted rotamers of triptycenes were separated by chromatography. Rotamers that carry an acetoxy, a hydroxy, or a t-butoxy substituent were prepared." @default.
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- W2034578045 date "1994-11-01" @default.
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- W2034578045 title "Syntheses of Rotational Isomers of Substituted 9-<i>t</i>-Butyltriptycenes That Carry an Oxygen Substituent in<i>t</i>-Butyl Group and Outstanding Steric Effects Observed in the Synthesis of an Intermediate" @default.
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- W2034578045 doi "https://doi.org/10.1246/bcsj.67.3076" @default.
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