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- W2034604218 abstract "Several analytical methods have been developed in the last 20 years for the determination of organotin compounds in mussel tissue. These methods encompass a huge variety of different extraction methods of poorly known efficiency. The quantitative evaluation of the extraction efficiency of these methods has been hindered by the lack of mussel reference materials and the presence of other potential sources of errors such as derivatisation and purification steps. The extraction efficiencies of 12 selected methods for the analysis of butyl- and phenyltin compounds in mussel samples have been compared. The comparison was carried out by analysing a mussel tissue reference material (CRM 477) with certified and indicative values for butyltins and phenyltins, respectively, recently made available by the European Commission's Standards, Measurements and Testing Programme. Derivatisation, clean-up and analysis were rigorously the same in all the methods considered. The high homogeneity of the samples and the identical experimental conditions allowed comparison of the extraction efficiencies." @default.
- W2034604218 created "2016-06-24" @default.
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- W2034604218 date "2000-03-01" @default.
- W2034604218 modified "2023-10-06" @default.
- W2034604218 title "Comparison of twelve selected extraction methods for the determination of butyl- and phenyltin compounds in mussel samples" @default.
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- W2034604218 doi "https://doi.org/10.1016/s0165-9936(99)00199-5" @default.
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