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- W2034690344 abstract "Abstract The adsorption of hydrophobic chelating agents on macroporous solids allows the preparation of efficient chelating resins. The adsorption of 7-(4-ethyl-methyloctyl)-8-quinolinol (Kelex 100), a selective reagent for gallium(III) and germanium(IV), on the macroreticular support Amberlite XAD-7 is studied in the present work by use of magic-angle spinning 13C NMR techniques. The solid-state NMR study is complemented by a short investigation based on FT-IR spectroscopy. It is concluded that the 7-(4-ethyl-1-methyloctyl)-8-quinolinol molecules are anchored to the solid support by their alkyl chains. It is also shown that the degree of rigidity of the latter depends on whether the amount of 7-(4-ethyl-1-methyloctyl)-8-quinolinol is greater or less than that needed to form a monolayer on the surface of the resin." @default.
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- W2034690344 date "1987-03-01" @default.
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- W2034690344 title "Magic-angle carbon-13 NMR investigation of solvent-impregnated resins: Application to 7-(4-ethyl-1-methyloctyl)-8-quinolinol (Kelex 100) adsorbed on Amberlite XAD-7" @default.
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- W2034690344 doi "https://doi.org/10.1016/0167-6989(87)90188-7" @default.
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