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- W2034695204 abstract "Carbon monoxide-containing complexes formed from nickel carbonyl and F-ketones in donor solvents are stable at 25 °C and decompose on heating with little or no elimination of fluoride ion. However, treatment of one such complex with iodobenzene at 25 °C resulted in benzoylation at oxygen with a concomitant loss of fluoride. Fluoroketones bearing an α-chlorine atom, on the other hand, reacted with nickel carbonyl at moderate temperatures with the facile loss of chloride ion to form, sequentially, enolate, keto alcohol, 1,6-diketone and cyclic diol derivatives. Methyl trifiuoropyruvate has been shown to be a special case in which reductive dimerization to dimethyl 1,2-dihydroxy-1,2-bis(trifluoromethyl)succinate was induced by nickel carbonyl rather than simple complexation." @default.
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- W2034695204 date "1994-03-01" @default.
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- W2034695204 title "Reaction of chlorodifluoromethylketones with nickel carbonyl" @default.
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- W2034695204 doi "https://doi.org/10.1016/0022-1139(93)02922-2" @default.
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