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- W2034751330 abstract "The bipodal ligands 3,3,3′,3′-tetraethyl-1,1′-isophthaloylbis(thiourea), H2L1, and 3,3,3′,3′-tetra(n-butyl)-1,1′-isophthaloylbis(thiourea), H2L2, react with Ni(II) and Pd(II) to form exclusively 2:2 metallomacrocyclic cis-[Pd(L2-S,O)]2 and cis-[Ni(L1-S,O)]2 complexes in high yields. Purple-brown cis-[Ni(L1-S,O)]2 readily form green adducts cis-[Ni(L1-S,O)(X)2]2 (X is pyridine or 4-dimethylaminopyridine), in which two X molecules are axially bound to each Ni(II) atom. Thermogravimetric analysis of these adducts shows that cis-[Ni(L1-S,O)(X)2]2 revert back to the planar cis-[Ni(L1-S,O)]2 complexes on heating. The crystal structures of 3,3,3′,3′-tetraethyl-1,1′-isophthaloylbis(thiourea), cis-[Pd(L2-S,O)]2, cis-[Ni(L1-S,O)(pyridine)2]2 and cis-[Ni(L1-S,O)(4-dimethylamino-pyridine)2]2 are reported." @default.
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- W2034751330 date "2001-04-01" @default.
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- W2034751330 title "Self-assembly of 2:2 metallomacrocyclic complexes of NiII and PdII with 3,3,3′,3′-tetraalkyl-1,1′-isophthaloylbis(thioureas). Crystal and molecular structures of cis-[Pd(L2-S,O)]2 and the adducts of the corresponding NiII complexes: [Ni(L1-S,O)(pyridine)2]2 and [Ni(L1-S,O)(4-dimethylaminopyridine)2]2" @default.
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- W2034751330 doi "https://doi.org/10.1016/s0022-2860(00)00924-8" @default.
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