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- W2034779006 abstract "A previosly unknown ordered low-temperature phase Li5NCl2-II has been obtained from the disordered high-temperature phase Li5NCl2-I by slow cooling (100°/h), while prolonged annealing at 400°C resulted in a decomposition to Li4NCl and LiCl. Neutron powder diffraction data were collected for both compounds and analyzed by the Rietveld method of profile refinement. Li5NCl2-II crystallizes in the hexagonal rhombohedral space groupR3m,a=366.10 (3),c=2851.6 (3) pm with three formula units per unit cell. Its structure may be regarded as composed of lithium nitride-like [Li4N]+layers and rock-salt-like [LiCl2]−double-layers, stacked along the hexagonalcaxis. A redetermination of the Li2O-type structure of Li5NCl2-I indicates the presence of N–Cl short-range order." @default.
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- W2034779006 date "1997-04-01" @default.
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- W2034779006 title "Preparation and Crystal Structure of Ordered and Disordered Lithium Nitride Dichloride, Li5NCl2" @default.
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- W2034779006 doi "https://doi.org/10.1006/jssc.1997.7283" @default.
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