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- W2034798874 abstract "Abstract Diorganotin(IV)-complexes of the N -nitroso- N -phenylhydroxylaminates (hereinafter cupf), Et 2 Sn(cupf) 2 ( 1 ), Bu 2 Sn(cupf) 2 ( 2 ), {[Bu 2 Sn(cupf)] 2 O} 2 ( 3 ), t -Bu 2 Sn(cupf) 2 ( 4 ) and Oc 2 Sn(cupf) 2 ( 5 , 6 ) were prepared and characterised by FT-IR and Mossbauer spectroscopic measurements. The binding modes of the ligand were identified by FT-IR spectroscopy, and it was found that the ligand is coordinated in chelating or bridging mode to the organotin(IV) center. The 119 Sn Mossbauer and FT-IR studies support the formation of trans -O h ( 1 – 6 ) structures. The X-ray diffraction analysis of 4 revealed that the tin centre is in a skew-trapezoidal geometry defined by four donors derived from the cupferronato ligands and two carbon atoms from the tin-bound t butyl substituents. The 119 Sn NMR investigations indicate that in solution 4 retains its hexacoordinated nature." @default.
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- W2034798874 date "2007-07-01" @default.
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- W2034798874 title "Preparation and structural studies on diorganotin(IV) complexes of N-nitroso-N-phenylhydroxylaminates" @default.
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- W2034798874 doi "https://doi.org/10.1016/j.jorganchem.2007.04.003" @default.
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