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• W2034834998 abstract "Tricyclopentadienyltetrahydrofuranuranium(III), (η5-C5H5)3U·OC4H8, crystallizes in the centrosymmetric monoclinic space group P21/n with a 8.248(3), b 24.322(17), c 8.357(4) Å, β 101.29(5)°, V 1644.0 Å3 and ρ(calc) 2.04 g cm−1 for Z = 4 and mol.wt. 595.0. Diffraction data (Mo-Kα, 2θ(max) 45°) were collected on an Enraf-Nonius CAD4 diffractometer and the structure was refined to Rw(F) 4.7% for those 1530 reflections having I > 2σ(I). The molecule consists of a distorted tetrahedral arrangement of THF and (η5-C5H5) ligands with CpUCp angles in the range 110.4–122.4° and CpUO angles between 90.2 and 106.0°. Individual uranium-carbon distances range from 2.76(2) to 2.82(2) Å and average 2.79[1] Å. The uranium-oxygen distance of 2.551(10) Å suggests a 10-coordinate U3+ radius of 1.20 Å in this class of compounds." @default.
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• W2034834998 date "1983-10-01" @default.
• W2034834998 modified "2023-10-18" @default.
• W2034834998 title "Crystal and molecular structure of tricyclopentadienyltetrahydrofuranuranium(III), (η5-C5H5)3U·OC4H8" @default.
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• W2034834998 doi "https://doi.org/10.1016/0022-328x(83)80132-6" @default.
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