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- W2034852007 abstract "Cbo-Aminoacylemetine entstehen in guten Ausbeuten durch Umsetzung von symmetrischen Cbo-Aminosäureanhydriden mit dem Alkaloid und anschließende Hydrogenolyse der Schutzgruppe. Anhydridsynthese und Aminoacylierung lassen sich im Eintopfverfahren durchführen. Bei Einsatz der cyclischen Anhydride von Cbo-Asparaginsäure und Cbo-Glutaminsäure wird ein Gemisch der α- und β- bzw. α- und γ-Aminoacylemetine erhalten. α- und γ-Glutamin werden getrennt und zugeordnet. Aminoacylation of Emetine Cbo-Aminoacylemetines are obtained in good yields by the action of symmetric Cbo-aminoacid anhydrides on the alkaloid, the protecting group is then hydrogenolysed. The anhydride synthesis and the aminoacylation can be carried out together in one step. The cyclic anhydride of Cbo-aspartic acid and Cbo-glutamic acid leads to a mixture of α-, and β- or α- and γ-aminoacylemetine respectively. α- and γ-Glutamicacyl emetines are separated, and the structure determined." @default.
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- W2034852007 date "1970-01-01" @default.
- W2034852007 modified "2023-09-27" @default.
- W2034852007 title "Aminoacylierungen des Emetins" @default.
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- W2034852007 doi "https://doi.org/10.1002/ardp.19703030205" @default.
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