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- W2034871410 abstract "Three hundred and twenty samples from the 1999 UK harvest comprising wheat (201 samples), barley (106) and oats (13) were analysed for ochratoxin A and deoxynivalenol. A small number of organic samples was also obtained. Samples were collected from farms, central stores, mills, maltings and ports from across the UK from February to April 2000. Ochratoxin A and deoxynivalenol analysis was by affinity column clean up and high-performance liquid chromatography with fluorescence and ultraviolet light detection, respectively, with limits of detection of 0.2 and 20 μg kg−1. The survey found ochratoxin A at below 5 μg kg−1 in 97% of the samples indicating satisfactory storage conditions. The remaining 3% of the samples contained ochratoxin A at levels between 5.2 and 231 μg kg−1, but none of these samples was intended for human consumption. Deoxynivalenol was detected in 88% of all samples, with 83% below 100 μg kg−1; the maximum level was 600 μg kg−1. Twenty samples containing deoxynivalenol at or above 150 μg kg−1 by high-performance liquid chromatography were all confirmed by gas chromatography/mass spectrometry. Nivalenol was also detected by gas chromatography/mass spectrometry at levels of 50 μg kg−1 or higher in 18 of 20 samples where deoxynivalenol was confirmed." @default.
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- W2034871410 date "2004-02-01" @default.
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- W2034871410 title "Survey of ochratoxin A and deoxynivalenol in stored grains from the 1999 harvest in the UK" @default.
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- W2034871410 doi "https://doi.org/10.1080/02652030310001648180" @default.
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