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- W2034891029 abstract "Abstract Three novel sandwich‐type polyoxotungstates ( 1 – 3 ) were synthesized in good yield using an in‐situ conventional solution synthesis method by reaction in aqueous media below 80 °C. Compounds 1 – 3 represent the first structurally characterized β ‐B‐BiW 9 sandwich‐type polyoxometalates with triethanolamine cations. All three compounds have the same building unit [( X (H 2 O) 3 ) 2 ( X 0.5 W 0.5 O) 2 ( β ‐B‐BiW 9 O 33 ) 2 )] 10– [ X = Mn II ( 1 ), Co II ( 2 ), Ni II ( 3 )]. The adjacent units of 1 or 2 are joined by Na + cations in different ways to construct 1D chains or 2D sheets. A 3D supramolecular structure is further formed by hydrogen bond interactions among water molecules and protonated triethanolamine cations. Meanwhile only compound 3 shows a 0D structure. The compounds were characterized by elemental analysis, IR spectroscopy, TG analysis, and single‐crystal X‐ray diffraction. Magnetic measurements on a sample of 1 show the presence of paramagnetic interactions." @default.
- W2034891029 created "2016-06-24" @default.
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- W2034891029 date "2010-05-20" @default.
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- W2034891029 title "Synthesis, Structure, and Magnetic Properties of Three Novel Sandwich-type Tungstobismuthates with Triethanolamine" @default.
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- W2034891029 doi "https://doi.org/10.1002/zaac.201000011" @default.
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