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- W2034898077 abstract "Abstract A new nonlinear optical semiorganic crystal, benzyltributylammonium trichlorobarium(II) monohydrate was grown by slow evaporation solution growth method at ambient temperature. The powder X-ray diffraction pattern of the crystal confirms its crystallinity. The absorption spectrum of the material shows a peak at 265 nm and no absorption observed in the entire visible region indicates that the compound can be used as a nonlinear optical material. The optical transmittance spectrum of the grown crystal shows a lower cut-off wavelength at 235 nm with transparency of 88%. Thermal stability of the crystal was studied by thermogravimetry-differential thermogravimetry and differential thermal analyses (TG-DTG and DTA). The differential scanning calorimetry (DSC) analysis shows thermal anomalies in the heating and cooling cycles that indicates the occurrence of a first order phase transition. The various characteristics absorption chemical bands and BaCl 3 − vibration were assigned through fourier transform infrared (FTIR) spectral analysis. The second harmonic generation efficiency (SHG) of the grown crystal was analyzed by Kurtz–Perry powder technique using Nd:YAG laser. The dielectric constant and dielectric loss of the compound decrease with increase in frequency." @default.
- W2034898077 created "2016-06-24" @default.
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- W2034898077 date "2014-01-01" @default.
- W2034898077 modified "2023-09-26" @default.
- W2034898077 title "Synthesis, spectral, thermal and optical characterization of benzyltributylammonium trichlorobarium(II) monohydrate crystal" @default.
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- W2034898077 doi "https://doi.org/10.1016/j.ijleo.2013.06.025" @default.
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