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• W2034938450 endingPage "6383" @default.
• W2034938450 startingPage "6369" @default.
• W2034938450 abstract "A marine polyether natural product okadaic acid is known to be a potent and specific inhibitor of protein phosphatases 1 and 2A. Herein, concise synthesis of the C15–C38 fragment of okadaic acid is reported. We investigated two different strategies for the construction of two spiroacetal substructures found in the target compound. The first strategy involved Suzuki–Miyaura coupling for the synthesis of endocyclic enol ethers and subsequent spiroacetalization. The second strategy exploited Suzuki–Miyaura coupling for the synthesis of exo-olefins as the precursor of spiroacetals. An alkynylaluminum–anomeric sulfone coupling effectively assembled the key spiroacetal substructures and completed the target compound." @default.
• W2034938450 created "2016-06-24" @default.
• W2034938450 creator A5059546479 @default.
• W2034938450 creator A5077476218 @default.
• W2034938450 creator A5084478484 @default.
• W2034938450 creator A5089771972 @default.
• W2034938450 date "2015-09-01" @default.
• W2034938450 modified "2023-10-12" @default.
• W2034938450 title "Concise synthesis of the C15–C38 fragment of okadaic acid, a specific inhibitor of protein phosphatases 1 and 2A" @default.
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• W2034938450 doi "https://doi.org/10.1016/j.tet.2015.04.001" @default.
• W2034938450 hasPublicationYear "2015" @default.

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