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- W2034959979 abstract "A novel trivalence dysprosium(Dy3+)-sensitized chemiluminescence method was developed for the first time for the determination of enoxacin (ENX) using flow-injection sampling based on the chemiluminescence (CL) associated with the reaction of the Dy3+-cerium(Ce(IV))-S2O32−-ENX system and the Dy3+-MnO4− S2O32−-ENX system. The analytical conditions for CL emission were investigated and optimized. The relationship between the CL intensity of ENX and its concentration has good linearity, with a correlation coefficient of 0.9984–0.9994. The limit of detection (LOD, 3σ) was 0.20 ng/mL for the Dy3+-ENX-S2O32−-Ce(IV)-H2SO4 system and 0.22 ng/mL for the Dy3+-ENX-S2O32−-MnO4−-HNO3 system. The relative standard deviation (RSD, n = 11) was 1.8% for 11 determinations of 60 ng/mL ENX. The proposed method was applied to the analysis of ENX in injections, serum and urine samples with a recovery of 98%–105%. A possible mechanism for this sensitized CL reaction is discussed by comparing the CL spectra with the fluorescence emission spectra. The proposed method represents a wide linear range, high sensitivity and accuracy, and can be used for the routine determination of ENX in pharmaceutical preparations and biological fluids. Copyright © 2009 John Wiley & Sons, Ltd." @default.
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- W2034959979 date "2009-03-01" @default.
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- W2034959979 title "Dysprosium-sensitized chemiluminescence system for the determination of enoxacin in pharmaceutical preparations and biological fluids with flow-injection sampling" @default.
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- W2034959979 doi "https://doi.org/10.1002/dta.25" @default.
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