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- W2035001572 abstract "Proposals have appeared aiming at the removal of sulfur in fuels by means of adsorption processes. The molecular sieves, silicoaluminiumphosphates, type SAPO, have been presented as an excellent adsorbent, with a great thermal and hydrothermal stability, and the impregnation of metal have became the adsorption even more selective, as they are a crystalline microporous material, and its acidity reaches intermediate values between the zeolite and aluminophosphate (ALPO's). Therefore, researchers have been dedicated to synthesize mesoporous SAPO-5. This work aims to synthesize and characterize the Microporous (SAPO-5) and mesoporous (SAPO5M) with the addition of specific template (TPOD), supported with different levels of transition metals, Ni and/or Zn. Thus, were synthesized the SAPO-5 and the SAPO-5M by hydrothermal method. Characterization techniques such as X-ray diffraction (XRD) and Textural Analysis (N2 adsorption/desorption) were carried out. The results are promising since the material had a surface area increase of 195.2 m g to 229.8 m g, about 19%, and the BET area an increase of five times in the pore diameter, with the addition of the reagent to obtain higher porosity. It follows that the process of synthesis of SAPO-5 and SAPO-5M shows to be effective for increasing the area and pore volume and with this addition of the reagent to obtain the mesoporosity, did not alter the crystallinity nor the structure of the material." @default.
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- W2035001572 date "2015-01-01" @default.
- W2035001572 modified "2023-09-26" @default.
- W2035001572 title "SYNTHESIS AND CHARACTERIZATION OF MICROPOROUS/MESOPOROUS SAPO-5" @default.
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