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- W2035006419 abstract "Abstract A method to simultaneously determine film permeability and surface area coverage of electrochemically generated and overoxidized polypyrrole (PPY) films on platinum is presented. The method, similar to the Koutecky–Levich approach, is based on the rotating disk electrode but uses experimental data from bare and film-covered electrodes to compensate for deviations from ideality. We address the effects of polymer growth potential, electrolyte concentration, monomer concentration, enzyme concentration and film thickness in film permeability, substrate surface area coverage and film adhesion of polypyrrole films grown from aqueous solutions. Film thickness was measured using transmission electron microscopy of films deposited on thin platinum wires. Surface morphology is illustrated using scanning electron micrographs. Relevant effects of film permeability and thickness are related to the response of amperometric polypyrrole-enzyme biosensors found in the literature." @default.
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- W2035006419 date "2004-04-01" @default.
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- W2035006419 title "Simultaneous determination of film permeability to H2O2 and substrate surface area coverage of overoxidized polypyrrole" @default.
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- W2035006419 doi "https://doi.org/10.1016/j.synthmet.2003.07.003" @default.
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