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• W2035100977 startingPage "1671" @default.
• W2035100977 abstract "We have determined elemental compositions for hundreds of components of diesel fuel, jet fuel (JP-8), and gasoline and characterized each of their chemical compositions before and after artificial “weathering” (i.e., evaporation to a specified fraction of the original weight). An all-glass heated inlet system (AGHIS) coupled to a home-built 6.0 T Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometer provides ultrahigh mass resolving power (m/Δm50% > 100 000, in which Δm50% is the full peak width at half-maximum peak height) and sufficiently high mass accuracy (≤0.8 ppm) for unique identification of all chemical components. A 1 μL septum injection of each weathered/unweathered transportation fuel into the AGHIS yields a mass spectrum containing 100−500 peaks, 50 ≤ m/z ≤ 300, with as many as five peaks (of different elemental composition) at a given nominal mass. Elemental composition assignment of every peak in the mass spectrum of each fuel and its weathered analogues provides a unique chemical “fingerprint” that serves to identify positively the contaminant and quantitate the extent of weathering. Weathered jet and diesel fuels (and gasoline to a lesser extent) exhibit a significant shift in the relative abundance to higher-mass (m/z ≥ 200) species, in accord with prior gas chromatographic (GC) evidence for a shift toward increased retention time with increased degree of weathering." @default.
• W2035100977 created "2016-06-24" @default.
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• W2035100977 date "2000-03-15" @default.
• W2035100977 modified "2023-09-29" @default.
• W2035100977 title "Complete Compositional Monitoring of the Weathering of Transportation Fuels Based on Elemental Compositions from Fourier Transform Ion Cyclotron Resonance Mass Spectrometry" @default.
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• W2035100977 doi "https://doi.org/10.1021/es990799i" @default.
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