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- W2035104278 abstract "The potentials of the bead injection scheme integrated into the sequential injection (SI) lab-on-valve (LOV) format, using reversed-phase materials for on-line matrix removal and analyte preconcentration, and interfaced with detection by electrothermal atomic absorption spectrometry (ETAAS), are exploited for the ultratrace determination of cadmium. The proposed approach relies upon the renewable surface concept and involves the incorporation of hydrophobic beads into channels of the LOV microconduit, thus serving as transient microcolumn packed reactors. After on-line analyte derivatization with diethyldithiophosphate (DDPA) in 1.3% (v/v) nitric acid medium, the resulting non-charged chelate is adsorbed onto the surface of the column material. The analyte loaded beads are afterwards eluted with 30 µl of ethanol which, via air segmentation, is subsequently introduced into the graphite tube for quantification. The used beads are then backflushed and delivered to waste. The ETAAS measurement is synchronized with the separation/preconcentration steps of the ensuing sample." @default.
- W2035104278 created "2016-06-24" @default.
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- W2035104278 date "2003-01-17" @default.
- W2035104278 modified "2023-10-01" @default.
- W2035104278 title "Exploiting the bead-injection approach in the integrated sequential injection lab-on-valve format using hydrophobic packing materials for on-line matrix removal and preconcentration of trace levels of cadmium in environmental and biological samples via formation of non-charged chelates prior to ETAAS detection" @default.
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- W2035104278 doi "https://doi.org/10.1039/b212024k" @default.
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