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- W2035164919 abstract "The crystal and molecular structures of the title compounds, [PtCl3(C3H8N)] (I), [PtCl3(C4H10N)] (II), and [PtCl3(C6H14N)] (III) have been determined by single-crystal X-ray methods. I crystallizes in the orthorombic system (Pbca) with a 10.444(3), b 8.782(2), c 17.036(5)Å, Z 8; II is monoclinic (P21/n) with a 7.953(5), b 11.254(6), c 10.722(6)Å, β 111.07(4)°, Z 4; III is orthorombic (P212121) with a 17.080(6), b 6.768(2), c 9.541(4)Å, Z 4. Full-matrix least-squares refinements have given final R-factors of 0.051 (1077 reflections for I), 0.043 (1325 reflections for II) and 0.041 (1123 reflections for III). The reflections were collected by counter methods and only those having I τ 3σ(I) were used in the analyses. In all three complexes platinum is four-coordinate, having as ligands the three chlorine atoms and the double bond of the(n=1, 2 or 4) cationic species. The structures are discussed, and compared with that of the analogous complex containing the pent-4-enylammonium cation,." @default.
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- W2035164919 date "1977-12-01" @default.
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- W2035164919 title "Crystal and molecular structures of the olefin complexes trichloro(π-allylammonium)platinum(II), trichloro(π-but-3-enylammonium)platinum(II) and trichloro(π-hex-5-enylammonium)platinum(II)" @default.
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- W2035164919 doi "https://doi.org/10.1016/s0022-328x(00)88355-2" @default.
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