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• W2035205562 abstract "A fast method for the determination of brominated flame retardants (BFRs) in styrenic polymers using microwave-assisted extraction (MAE) and liquid chromatography with UV detection (HPLC–UV) was developed. Different extraction parameters (extraction temperature and time, type of solvent, particle size) were first optimised for standard high-impact polystyrene (HIPS) samples containing known amounts of tetrabromobisphenol A (TBBPA) and decabromodiphenyl ether (Deca-BDE). Complete extraction of TBBPA was achieved using a combination of polar/non-polar solvent system (isopropanol/n-hexane) and high extraction temperatures (130 °C). Lower extraction yields were, however, obtained for Deca-BDE, due to its high molecular weight and its non-polar nature. The developed method was successfully applied to the screening of BFRs in standard plastic samples from waste electrical and electronic equipment (WEEE); TBBPA could be fully recovered, and Deca-BDE could be identified, together with minor order polybrominated diphenyl ether (PBDE) congeners." @default.
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• W2035205562 date "2009-04-15" @default.
• W2035205562 modified "2023-10-14" @default.
• W2035205562 title "Microwave-assisted extraction for qualitative and quantitative determination of brominated flame retardants in styrenic plastic fractions from waste electrical and electronic equipment (WEEE)" @default.
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• W2035205562 doi "https://doi.org/10.1016/j.talanta.2008.10.038" @default.
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