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- W2035321172 abstract "Glycosides of 2-acetamido-2-deoxy- d -glucopyranose were treated with triphenylphosphine and N -bromosuccinimide to form the 6-bromo-6-deoxy derivatives. These, on hydrogenolysis in the presence of a palladium catalyst, yielded glycosides of 2-acetamido-2,6-dideoxy- d -glucopyranose ( N -acetyl- d -quinovosamine). When the benzyl β- d -glycoside was the starting material, the product was free N -acetyl- d -quinovosamine. The allyl 6-bromo-6-deoxy-α- and -β-glycosides, after partial benzoylation, were reduced by tributyltin hydride to allyl 2-acetamido-3- O -benzoyl-2,6-dideoxy-α- and -β- d -glucopyranoside. The α anomer was converted into allyl 2-acetamido-2,6-dideoxy-α- d -galactopyranoside (α glycoside of N -acetyl- d -fucosamine) by successive trifluoromethylsulfonylation, displacement with cesium benzoate, and O -debenzoylation." @default.
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- W2035321172 date "1983-08-01" @default.
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- W2035321172 title "A convenient preparation of 2-acetamido-2,6-dideoxy-d-glucose, some of its alkyl glycosides, and allyl 2-acetamido-2,6-dideoxy-α-d-galactopyranoside" @default.
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- W2035321172 doi "https://doi.org/10.1016/0008-6215(83)84057-9" @default.
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