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- W2035437199 abstract "Tetrabutylammonium fluoride (TBAF) is prepared at low temperature by nucleophilic aromatic substitution of hexafluorobenzene with tetrabutylammonium cyanide. Adventitious water is scavenged during this synthesis by the generated hexacyanobenzene, which readily adds water under basic conditions. Contrary to expectations, TBAF is stable to Hofmann elimination in polar aprotic solvents under anhydrous conditions. Added hydroxylic solvents are shown to catalyze the decomposition of TBAF and to catalyze proton exchange with DMSO. The synthetic utility of this salt is described briefly." @default.
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- W2035437199 date "2005-01-28" @default.
- W2035437199 modified "2023-10-16" @default.
- W2035437199 title "Anhydrous Tetrabutylammonium Fluoride" @default.
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- W2035437199 doi "https://doi.org/10.1021/ja0440497" @default.
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