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- W2035587883 abstract "The title complex, [(C(4)H(9))(4)N](2)[Mo(6)(C(7)H(6)ClN)O(18)], was prepared by the reaction of (Bu(4)N)(4)[α-Mo(8)O(26)] and 2-methyl-5-chloro-aniline hydro-chloride with N,N'-dicyclo-hexyl-carbodiimide as dehydrating agent in dry acetonitrile solution. The aryl-imido ligand is linked to an Mo atom of the Lindqvist-type hexamolybdate anion by an Mo N triple bond, with a bond length of 1.732 (4) Å and an Mo N-C bond angle of 169.1 (4)°, typical for monodentate imido groups in such hybrid complexes. Due to the inter-action between one H atom in the aryl group and an O atom of a symmetry-related hexa-molybdate cluster, the anions form centrosymmetric dimers in the crystal structure. Weak C-H⋯O contacts are observed between the cations and anions. Unresolved disorder in some of the butyl chains of the ammonium cation is noted." @default.
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- W2035587883 date "2011-09-20" @default.
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- W2035587883 title "A new mono-functionalized organoimido hexamolybdate derivative: bis(tetra-<i>n</i>-butylammonium) (5-chloro-2-methylphenylimido)-μ<sub>6</sub>-oxido-dodeca-μ<sub>2</sub>-oxido-pentaoxidohexamolybdate(VI)" @default.
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- W2035587883 doi "https://doi.org/10.1107/s1600536811036063" @default.
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