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- W2035604800 abstract "An efficient synthesis of β-d-GlcpNAc-(1→3)-α-l-Rhap-(1→2)-[β-l-Xylp-(1→4)]-α-l-Rhap-(1→3)-α-l-Rhap, the repeating unit of the O-antigen produced by Pseudomonas solanacearumICMP7942 and its isomer β-d-GlcpNAc-(1→3)-α-l-Rhap-(1→4)-[β-l-Xylp-(1→2)]-α-l-Rhap-(1→3)-α-l-Rhap was achieved via sequential assembly of the building blocks, allyl 2,3-O-isopropylidene-α-l-rhamnopyranoside (2), allyl 3,4-O-isopropylidene-α-l-rhamnopyranoside (3), allyl 2,4-di-O-benzoyl-α-l-rhamnopyranoside (6), 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-d-glucopyranosyl trichloroacetimidate (7), and 2,3,4-tri-O-benzoyl-β-l-xylopyranosyl trichloroacetimidate (12). The process was carried out in a regio- and stereoselective manner using glycosyl trichloroacetimidates as donors and unprotected or partially protected rhamnopyranosides as acceptors in the presence of a catalytic amount of trimethylsilyl trifluoromethanesulfonate (TMSOTf)." @default.
- W2035604800 created "2016-06-24" @default.
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- W2035604800 date "2003-01-01" @default.
- W2035604800 modified "2023-09-27" @default.
- W2035604800 title "Synthesis of β-d-GlcpNAc-(1→3)-α-l-Rhap-(1→2)-[β-l-Xylp-(1→4)]-α-l-Rhap-(1→3)-α-l-Rhap, the repeating unit of the O-antigen produced by Pseudomonas solanacearumICMP 7942" @default.
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- W2035604800 doi "https://doi.org/10.1016/s0008-6215(02)00358-0" @default.
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