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• W2035698355 abstract "The polymorphism of (CH3)3CCl has been further investigated by both thermal and X-ray powder diffraction experiments. From the former, the phase transitions between the different phases (IV, III, II, I, and L) have been thermally characterized, and in particular, the temperature domain of phase II has been settled to be from 217.9 to 219.8 K by means of Cp measurements. The structure of the lowest-temperature phase IV of (CH3)3CCl has been determined by X-ray powder diffraction and Rietveld profile refinement. The structure, P21/m with two molecules per unit cell, has been found to be isostructural with that of phase II of (CH3)3CCN. The intermolecular interactions in the solid-state phases for (CH3)3CCl as well as for (CH3)3CCN have been analyzed by the study of the isobaric thermal-expansion tensor. The anisotropy of such interactions are discussed in the light of the previously studied dynamics disorder." @default.
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• W2035698355 date "2000-01-22" @default.
• W2035698355 modified "2023-09-27" @default.
• W2035698355 title "Thermal and Structural Characterization of (CH₃)₃CCl" @default.
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• W2035698355 doi "https://doi.org/10.1021/cm9911565" @default.
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