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- W2035736699 abstract "Temperature-programmed desorption (TPD) of self-assembled monolayers (SAMs) on gold is investigated by using in parallel mass spectrometry (MS) and infrared reflection−absorption spectroscopy (IRAS). Monolayers formed by HS(CH2)n−OH (n = 18, 22) and HS(CH2)15−CONH−(CH2CH2O)−H (EG1) are compared to reveal the influence of specifically introduced hydrogen-bonding groups on their thermal stability. The overall desorption process of the above molecules is found to occur in two main steps; a disordering of the alkyl chains followed by a complex series of decomposition/desorption reactions. The final step of the process involves desorption of sulfur from different chemisorption states. The amide-group-containing SAM, which is stabilized by lateral hydrogen bonds, displays a substantial delay of the alkyl chain disordering by about 50 K, as compared to the linear chain alcohols HS(CH2)n−OH. Moreover, the decomposition of the alkyls and the onset of sulfur desorption occur at a temperature that is higher by appro..." @default.
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- W2035736699 date "2002-09-12" @default.
- W2035736699 modified "2023-10-14" @default.
- W2035736699 title "Thermal Stability of Self-Assembled Monolayers: Influence of Lateral Hydrogen Bonding" @default.
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- W2035736699 doi "https://doi.org/10.1021/jp0200526" @default.
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