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- W2035754634 abstract "Abstract The compounds BaLiB9O15 (BaLi), BaNaB9O15 (BaNa) and SrLiB9O15 (SrLi) have been synthesised, and their structure determined by single crystal X-ray diffraction methods. Each borate crystallises with six formula units in the R3c non-centrosymmetric space group. Cell parameters are: a=11.0223(19) A, c=17.106(4) A, and V=1799.8(6) A3 for the (BaLi) compound; a=11.0933(15) A, c=17.392(3) A, and V=1853.5(5) A3 for the (BaNa) compound; a=10.6129(9) A, c=17.555(2) A, and V=1712.4(3) A3 for (SrLi) compound. The borate anion is characterised by a three-dimensional framework built up from [B3O7] rings; its shorthand notation is 3: ∞3 (2△+T), where △ is a BO3 triangle and T is a BO4 tetrahedron. In these three compounds, the alkaline earth (Ba, Sr) and the alkaline (Li, Na) ions occupy alternate sites in the channels along the c axis; however, their oxygenated environment is different. In (BaNa) and (SrLi), the [BaO9] and [SrO9] form tricapped trigonal prisms and [NaO6] and [LiO6] trigonal antiprisms whereas in (BaLi), [BaO12] forms an irregular icosahedron and there are only three oxygen atoms in the neighboring of lithium ion." @default.
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- W2035754634 date "2001-11-01" @default.
- W2035754634 modified "2023-10-16" @default.
- W2035754634 title "Synthesis and crystal structure of three MM′B9O15 borates (M=Ba, Sr and M′=Li; M=Ba and M′=Na)" @default.
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- W2035754634 doi "https://doi.org/10.1016/s1466-6049(01)00078-2" @default.
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