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• W2035804904 abstract "A fast and direct determination procedure for precious metals in spent automotive catalyst was developed using the novel high-energy polarized-beam XRF. A sample preparation method working directly on the ground material was optimized. The material was pressed as a pellet using wax as a binder; no internal standard was added. The standards for this application were available spent automotive catalyst, previously analyzed by ICP-OES to verify their concentration, prepared in the same way as the unknown samples. The investigated concentration ranged from nearly 0 to approximately 2700 ppm for Pt, to 500 ppm for Rh, and to 7500 ppm for Pd. The repeatability of the XRF measurement appeared to be better than 0.5%, while the precision of the whole method was ∼1%. The accuracy of the XRF method was verified with the well-established (but very time-consuming) ICP-OES method; a good agreement (no difference when using the 95% confidence interval) was found for the results. When using an irradiation time of 500 s for the CsI secondary target and the Zr secondary target, the detection limits for Pt, Pd, and Rh were found to be better than 5 ppm." @default.
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• W2035804904 date "2007-07-13" @default.
• W2035804904 modified "2023-10-12" @default.
• W2035804904 title "Determination of Platinum, Palladium, and Rhodium in Automotive Catalysts Using High-Energy Secondary Target X-ray Fluorescence Spectrometry" @default.
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• W2035804904 doi "https://doi.org/10.1021/ac070815r" @default.
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