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- W2035862321 abstract "When Ca glycolate is mixed with H 3 PO 4 in a Ca/P ratio of 1.67 containing acetic acid contents in a range of HOAC/Ca ratios from zero to six, the as-prepared mixtures have fine particles. The as-prepared mixtures are transformed to precipitates or solution depending on the HOAC contents and the amount of stirring. If the as-prepared mixtures are further stirred for 8 h, precipitation occurs for all mixtures with various HOAC contents. If an as-prepared mixture has a HOAC/Ca ratio of six, without further stirring it can become a solution after being kept for one day, and the solution is transformed to a transparent gel after keeping for 20 h. The transparent gel is transformed to a poorly developed hydroxyapatite phase after drying at 150 °C for 24 h and to a pure and well-developed hydroxyapatite phase after calcining at above 750 °C for 1 h. HOAC in the mixtures is suggested to play a role in retarding the reactions between Ca glycolates and H 3 PO 4 , and the critical role of stirring in forming a transparent gel is proposed as the occurrence of a heterogeneous reaction process in the system." @default.
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- W2035862321 date "1998-09-01" @default.
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- W2035862321 title "The sol-gel process in the 5Ca glycolate-3H3PO4 system" @default.
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- W2035862321 doi "https://doi.org/10.1016/s0254-0584(98)00129-1" @default.
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