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- W2035925141 abstract "The reaction of m-terphenyl amine (2,6-bis-(2,4,6-trimethylphenyl)aniline, m-Ter = m-terphenyl = 2,6-bis-(2,4,6-trimethylphenyl)) and ECl3 (E = P, As) in the presence of different bases (Et3N, n-BuLi, LDA, DBU) and under different reaction conditions was studied. The reaction with excess Et3N yielded m-Ter–N(H)–AsCl2 for E = As, while for E = P m-Ter–N(PCl2)2 was formed. m-Ter–N(H)–ECl2 was obtained in the reaction of m-terphenyl amine with n-BuLi and ECl3 for E = As and P. Further treatment of m-Ter–N(H)–PCl2 with Et3N led to the formation of 1,3-dichloro-cyclo-1,3-diphospha-2,4-diazane, a synthesis protocol which cannot be applied to the analogous arsenic species. 1,3-dichloro-cyclo-1,3-diarsa-2,4-diazane was isolated when DBU was added to m-Ter–N(H)–AsCl2 at low temperature (−80 °C)." @default.
- W2035925141 created "2016-06-24" @default.
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- W2035925141 date "2010-01-01" @default.
- W2035925141 modified "2023-10-07" @default.
- W2035925141 title "Synthesis of sterically encumbered 2,4-bis-m-terphenyl-1,3-dichloro-2,4-cyclo-dipnictadiazanes [m-TerNPnCl]2, (Pn = P, As)" @default.
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- W2035925141 doi "https://doi.org/10.1039/c0dt00700e" @default.
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